| Identification | Back Directory | [Name]
2-ACETYL-6-METHOXYPYRIDINE 97 | [CAS]
21190-93-2 | [Synonyms]
2-Acetyl-6-methoxypyridine
2-Acetyl-6-Methoxypyridine 97%
2-ACETYL-6-METHOXYPYRIDINE 97
2-Acetyl-6-methoxypyridine >
1-(6-Methoxypyridin-2-yl)ethanone
Ethanone, 1-(6-methoxy-2-pyridinyl)-
1-(6-Methoxypyridin-2-yl)ethan-1-one | [Molecular Formula]
C8H9NO2 | [MDL Number]
MFCD08276836 | [MOL File]
21190-93-2.mol | [Molecular Weight]
151.164 |
| Chemical Properties | Back Directory | [Melting point ]
40-44 °C
| [Boiling point ]
85 °C0.2 mm Hg
| [density ]
1.093±0.06 g/cm3(Predicted) | [Fp ]
202 °F
| [storage temp. ]
Inert atmosphere,Room Temperature | [solubility ]
soluble in Methanol | [form ]
powder to crystal | [pka]
1.72±0.10(Predicted) | [color ]
White to Light yellow to Light orange |
| Hazard Information | Back Directory | [Synthesis]
GENERAL METHODS: A mixture of 2-methoxypyridine (1c, 0.216 mg, 2 mmol) and acetyl chloride (2a, 0.157 mg, 2 mmol) was mixed with CTAB/CTAC (0.001 mol) in 1,2-dichloroethane. The resulting reaction mixture was heated in a controlled microwave synthesizer (Biotage Initiator+ SP Wave model, 0.200 W, 2.45 GHz, with an additional 60 W at steady state) for 5 min under reaction conditions of 100 °C and 2 bar pressure. Upon completion of the reaction, the target product 2-acetyl-6-methoxypyridine (3o) was isolated by column chromatography using ethyl acetate-petroleum ether as eluent for purification on silica gel. | [References]
[1] Tetrahedron Letters, 2013, vol. 54, # 26, p. 3431 - 3436 |
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| Company Name: |
Energy Chemical
|
| Tel: |
021-021-58432009 400-005-6266 |
| Website: |
http://www.energy-chemical.com |
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