1,1'-Bis(di-tert-butylphosphino)ferrocene synthesis
- Product Name:1,1'-Bis(di-tert-butylphosphino)ferrocene
- CAS Number:84680-95-5
- Molecular formula:C26H44FeP210*
- Molecular Weight:474.42
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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Yield:-
Reaction Conditions:
in hexanecomplex suspended in hexane, chlorodi-tert-butylphosphine added at -78°C, allowed to warm to room temp., stirred for 2 h; hydrolyzed with H2O, hexane layer sepd., dried (MgSO4), filtered, concd., chromd. (Al2O3, petroleum ether/Et2O), solvent removed, obtained impure;
References:
Cullen, William R.;Kim, Tae-Jeong;Einstein, Frederick W. B.;Jones, Terry [Organometallics,1983,vol. 2,# 6,p. 714 - 719]