6-Chloro-1H-indazole-5-carboxylic acid methyl ester synthesis
- Product Name:6-Chloro-1H-indazole-5-carboxylic acid methyl ester
- CAS Number:1372629-24-7
- Molecular formula:C9H7ClN2O2
- Molecular Weight:210.62
67-56-1
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Yield:1372629-24-7 19%
Reaction Conditions:
with 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl;triethylamine;palladium dichloride in acetonitrile at 100; under 30003 Torr; for 18 h;
References:
Wainwright, Philip;Perni, Remedios;Vickers, Clare;Coffey, Steven B.;Buzon, Leanne;Dirico, Kenneth;Nelson, Kendra L.;Zhao, Zhengrong;Limberakis, Chris;Freeman-Cook, Kevin D.;Corbett, Jeffrey W. [Synthetic Communications,2012,vol. 42,# 13,p. 1914 - 1921] Location in patent:experimental part