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52074-51-8

2,4,6-Trichloro-3,5-difluoropyridine synthesis

1synthesis methods
-

Yield:52026-98-9 7% ,54889-43-9 1% ,52074-51-8 9%

Reaction Conditions:

in sulfolane;bomb tube; first at 50-80 °C (17 h), then at 110-130 °C (135 h);;

References:

Chambers, R. D.;Hole, M.;Musgrave, W. K. R.;Thorpe, J. G. [Journal of the Chemical Society C: Organic][Journal of the Chemical Society [Section] C: Organic,1971,p. 61 - 67]

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