2,6-DICHLOROPHENETHYLALCOHOL synthesis
- Product Name:2,6-DICHLOROPHENETHYLALCOHOL
- CAS Number:30595-79-0
- Molecular formula:C8H8Cl2O
- Molecular Weight:191.05
54551-83-6
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30595-79-0
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Yield:-
Reaction Conditions:
with sodium tetrahydroborate in tetrahydrofuran;water at 5 - 10; for 4 h;
Steps:
1
2,6-Dichloro phenyl acetic acid methyl ester (1 eq) was taken in THF: Water (10:0.1(v/v) and cooled to 5-10 0C. NaBH4 was added to this mixture and mixture was stirred for 4 h. Mixture was quenched in water and extracted with EtOAc. Organic layer was washed with brine and evaporated in vacuo to afford title compound as thick liquid.
References:
CADILA HEALTHCARE LIMITED WO2009/87649, 2009, A1 Location in patent:Page/Page column 23
6575-24-2
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30595-79-0
142 suppliers
$8.00/250mg