2-Ethylhexyl glycidyl ether synthesis
- Product Name:2-Ethylhexyl glycidyl ether
- CAS Number:2461-15-6
- Molecular formula:C11H22O2
- Molecular Weight:186.29
104-76-7
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Yield:-
Reaction Conditions:
Stage #1: 2-Ethylhexyl alcoholwith tetrabutylammomium bromide;sodium hydroxide at -40; for 0.5 h;Inert atmosphere;
Stage #2: epichlorohydrin at 40; for 12 h;Reagent/catalyst;Temperature;
Steps:
1 Optimization of production process of 2-ethylhexyl glycidyl ether
1 mol of 2-ethylhexanol, 2 mol of NaOH and 0.005 mol of tetra-n-butyl ammoniumbromide (TBAB) were charged and stirred for 30 minutes at 40 ° C under a nitrogen atmosphere. Then, 2 mol of epichlorohydrin (ECH) was added dropwise at 40 ° C for 30 minutes using a metering pump, and reacted at different reaction temperatures for 12 hours. The reaction was then analyzed by GC to compare the reactivity with the reaction temperature. The experimental conditions and experimental results are shown in Table 1 below.
References:
KR101528751,2015,B1 Location in patent:Paragraph 0047-0051
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2461-15-6
228 suppliers
$30.00/25mL
104-76-7
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$5.00/10g
106-89-8
771 suppliers
$9.00/10g
2461-15-6
228 suppliers
$30.00/25mL
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