3-BROMO-2-BENZYLAMINOPYRIDINE synthesis
- Product Name:3-BROMO-2-BENZYLAMINOPYRIDINE
- CAS Number:868603-37-6
- Molecular formula:C12H11BrN2
- Molecular Weight:263.13
Yield:868603-37-6 90%
Reaction Conditions:
Stage #1: 2-Amino-3-bromopyridinewith sodium hydride in tetrahydrofuran at 0 - 40; for 0.5 h;Inert atmosphere;
Stage #2: benzyl bromide in tetrahydrofuran at 0 - 60; for 1 h;Inert atmosphere;
References:
Vrijdag, Johannes L.;De Ruysscher, Dries;De Borggraeve, Wim M. [European Journal of Organic Chemistry,2017,vol. 2017,# 11,p. 1465 - 1474]
54231-33-3
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100-46-9
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868603-37-6
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54231-40-2
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3723-70-4
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