3-methylcyclopent-2-en-1-one synthesis
- Product Name:3-methylcyclopent-2-en-1-one
- CAS Number:2758-18-1
- Molecular formula:C6H8O
- Molecular Weight:96.13
110-13-4
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2758-18-1
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Yield:2758-18-1 98%
Reaction Conditions:
with calcium(II) oxide in lithium hydroxide monohydrate at 150; for 14 h;Inert atmosphere;Reagent/catalyst;Temperature;Solvent;
Steps:
1-20 Example 1
3g of 2,5-hexanedione and 10mL of water were added to a 25mL three-necked flask. Under an inert atmosphere (selected nitrogen), the temperature was increased to 150 ° C, and then 400mg of CaO was added. After 14 hours of reaction, the product was analyzed by gas chromatography. The yield of methylcyclopentenone reached 98%.
References:
CN110550993,2019,A Location in patent:Paragraph 0048-0052
59078-89-6
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2758-18-1
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![6-Oxabicyclo[3.1.0]hexan-2-one,5-methyl-](/CAS/20180527/GIF/17024-44-1.gif)
17024-44-1
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2758-18-1
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