ChemicalBook CAS DataBase List 4-METHOXY-4-METHYL-2-PENTANONE

4-METHOXY-4-METHYL-2-PENTANONE synthesis

7synthesis methods

Product Name:4-METHOXY-4-METHYL-2-PENTANONE
CAS Number:107-70-0
Molecular formula:C7H14O2
Molecular Weight:130.18

52-90-4 Synthesis

52-90-4
946 suppliers
$6.00/10g

38348-31-1
0 suppliers
inquiry

141-79-7 Synthesis

141-79-7
279 suppliers
$10.00/5g

109-49-9 Synthesis

109-49-9
128 suppliers
$12.00/1g

19872-52-7
243 suppliers
$5.00/100mg

123-42-2 Synthesis

123-42-2
593 suppliers
$19.00/100ml

107-70-0
69 suppliers
$35.00/25mL

124-38-9
130 suppliers
$175.00/23402

201230-82-2 Synthesis

201230-82-2
1 suppliers
inquiry

Yield:-

Reaction Conditions:

with air at 30 - 180;

Steps:

3.3. Experimental Procedures
General procedure: A temperature setting range of 30~180 °C was used in this paper for the low-temp oxidation experiments. The air flow is set to 20 mL/min. Firstly, the 6201 support with the attached organic sulfur model compound is put into the sample can, then the sample can is placed in the programmed temperature adjustment oven, and the air flow is set to 20 mL/min. Next, we turn on the programmed temperature adjustment oven which is heated in 10 °C temperature intervals. When the temperature of the can reaches the setting temperature, we hold that state for 20 min. After that, we analyze the gas composition using the chromatograph and infrared gas analyzer. When the temperature reaches 180 °C, then programmed temperature cycle is stopped and the oven is shut down. After waiting until the sample cools down to room temperature, the sample can is opened and 1 g of 6201 support is removed. Next, we put this 1 g of 6201 support into a breaker, and add 2 g of acetone. After mixing with a glass rod and allowing to stand for 20 min we use a dropper to transfer the extract liquor from the upper layer into a glass bottle, annotating and properly sealing it before using GC/MS to conduct component analysis.

References:

Zhang, Lanjun;Li, Zenghua;Li, Jinhu;Zhou, Yinbo;Yang, Yongliang;Tang, Yibo;McPhee, Derek J. [Molecules,2015,vol. 20,# 12,p. 22241 - 22256]

67-56-1 Synthesis