5,6-dimethyl-2-methylsulfanyl-1h-benzoimidazole synthesis
- Product Name:5,6-dimethyl-2-methylsulfanyl-1h-benzoimidazole
- CAS Number:35190-53-5
- Molecular formula:C10H12N2S
- Molecular Weight:192.28
Yield:35190-53-5 55.4%
Reaction Conditions:
with potassium carbonate in acetone; for 24 h;
Steps:
2.2.2 Synthesis of 2-(methylthio)-5,6-(un) substituted-1H-benzo[d]imidazoles (7-9)
General procedure: (0.01mol) of compounds 4-6, was stirred with methyl iodide (10ml), anhydrous potassium carbonate (1g) in 50ml acetone for 24h. The resultant solution was then evaporated under vacuum and the obtained residue was crystallized from aqueous ethanol to obtain the mentioned derivatives in reasonable yields.
References:
Elkot, Hoda A.;Ragab, Ibrahim;Saleh, Noha M.;Amin, Mohamed N.;Al-Rashood, Sara T.;El-Messery, Shahenda M.;Hassan, Ghada S. [Chemico-Biological Interactions,2021,vol. 344,art. no. 109530]
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