2,2'-bipyridine-5,5'-diamine synthesis
- Product Name:2,2'-bipyridine-5,5'-diamine
- CAS Number:52382-48-6
- Molecular formula:C10H10N4
- Molecular Weight:186.21
5350-93-6
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52382-48-6
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid / toluene / 5 h / 100 °C / Dean-Stark
2: zinc; dibromobis(triphenylphosphine)nickel(II); tetraethylammonium iodide / tetrahydrofuran / 60 °C / Inert atmosphere
3: hydroxylamine hydrochloride; triethylamine / water; ethanol / 44 h / Reflux
References:
Sun, Qi;Aguila, Briana;Perman, Jason;Nguyen, Nicholas;Ma, Shengqian [Journal of the American Chemical Society,2016,vol. 138,# 48,p. 15790 - 15796]
869781-58-8
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52382-48-6
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39858-84-9
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![Carbamic acid, N,N'-[[2,2'-bipyridine]-5,5'-diyl]bis-, C,C'-diethyl ester](/CAS/20240320/GIF/63361-69-3.gif)
63361-69-3
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52382-48-6
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13534-97-9
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52382-48-6
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