8-METHYLDECANOIC ACID synthesis

7synthesis methods

Product Name:8-METHYLDECANOIC ACID
CAS Number:5601-60-5
Molecular formula:C11H22O2
Molecular Weight:186.29

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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 8.05 g / SnCl₄ / CH₂Cl₂ / 2.5 h / 0 °C
2: 5.04 g / amalgamated zinc / acetic acid / 12 h / 20 °C
3: H₂ / Raney-Ni / propan-2-ol / 48 h
4: 3.35 g / 3 M NaOH / methanol; dioxane

References:

Hedenstroem, Erik;Nguyen, Ba-Vu;Silks III, Louis A. [Tetrahedron Asymmetry,2002,vol. 13,# 8,p. 835 - 844]

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References

2-Thiopheneacetic acid, 5-(2-methylbutyl)-, ethyl ester

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References

2-Thiopheneacetic acid, 5-(2-methyl-1-oxobutyl)-, ethyl ester

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References

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References

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8-METHYLDECANOIC ACID synthesis

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