TERT-BUTYL 4-(AMINOCARBONYL)TETRAHYDROPYRIDINE-1(2H)-CARBOXYLATE synthesis
- Product Name:TERT-BUTYL 4-(AMINOCARBONYL)TETRAHYDROPYRIDINE-1(2H)-CARBOXYLATE
- CAS Number:91419-48-6
- Molecular formula:C11H20N2O3
- Molecular Weight:228.29
39546-32-2
365 suppliers
$6.00/5g
24424-99-5
863 suppliers
$13.50/25G
91419-48-6
237 suppliers
$20.80/1G
Yield:91419-48-6 95%
Reaction Conditions:
with 4-methylmorpholine N-oxide in 1,4-dioxane;Product distribution / selectivity;
Steps:
1
The ring nitrogen atom of isonipecotamide 1 (commercially available from Aldrich) was Boc-protected in 95% isolated yield by using Boc20 in dioxane and NMO as the base.
References:
WO2004/2483,2004,A1 Location in patent:Page/Page column 21-22
84358-13-4
395 suppliers
$5.00/5g
91419-48-6
237 suppliers
$20.80/1G
124443-68-1
267 suppliers
$6.00/5g
91419-48-6
237 suppliers
$20.80/1G
![1-PIPERIDINECARBOXYLIC ACID,4-[(HYDROXYIMINO)METHYL]-,1,1-DIMETHYLETHYL ESTER](/CAS/GIF/190446-85-6.gif)
190446-85-6
32 suppliers
$60.00/100mg
91419-48-6
237 suppliers
$20.80/1G
24424-99-5
863 suppliers
$13.50/25G
91419-48-6
237 suppliers
$20.80/1G