Cyclohexylhydrazine hydrochloride synthesis
- Product Name:Cyclohexylhydrazine hydrochloride
- CAS Number:24214-73-1
- Molecular formula:C6H15ClN2
- Molecular Weight:150.65
60295-21-8
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24214-73-1
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Yield:24214-73-1 100%
Reaction Conditions:
with hydrogenchloride in 1,4-dioxane;Reflux;
Steps:
161.3 Example 161: 4-chloro-N-(4-chlorophenyl)-1-cyclohexyl-3-methyl-1H-pyrazolo [3,4-b]pyridine-5-carboxamide
General procedure: To a solution of tert-butyl 2-cyclohexylhydrazine-1-carboxylate (1 .9g, 8 .87mmol) in dioxane was added HCl/dioxane (20 mL), it was then refluxed overnight. The white precipitate was filtrated to afford 1.8g (yield:>100%) of cyclohexylhydrazine hydrochloride as a white solid.
References:
WO2016/123392,2016,A2 Location in patent:Paragraph 00476
67959-46-0
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24214-73-1
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24214-73-1
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24214-73-1
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