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ChemicalBook CAS DataBase List ISOBUTYL LACTATE
585-24-0

ISOBUTYL LACTATE synthesis

4synthesis methods
-

Yield:-

Reaction Conditions:

with tin-titanium-silicon molecular sieve at 60; for 7 h;

Steps:

4 Example 4
Weigh 0.15g of the tin-titanium-silicon molecular sieve Sn-Ti-MFI-4 provided in Preparation Example 4 as a catalyst and put it in a 15mL glass reaction tube, then add a magnetic stirrer, 8g isobutanol, and 0.1g pyruvaldehyde in sequence, and screw on Glass reaction tube lid. Put the glass reaction tube in the oil bath on the temperature-controlled magnetic stirrer, start the magnetic stirrer and heating device, and start the reaction. The reaction temperature was controlled at about 60°C and reacted for 7 hours. The specific reaction results are shown in Table 1.

References:

Sinopec Corporation;Sinopec Corporation Petrochemical Sciences Institute;Liu Yujia;Xia Changjiu;Zhao Yi;Peng Xinxin;Yang Yongjia;Lin Min;Zhu Bin;Luo Yibin;Shu Xingtian CN111253248, 2020, A Location in patent:Paragraph 0193; 0194; 0210

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