N-(4-BROMOPHENYL-N-(4-CARBETHOXYPHENYL)AMINE synthesis
- Product Name:N-(4-BROMOPHENYL-N-(4-CARBETHOXYPHENYL)AMINE
- CAS Number:458550-44-2
- Molecular formula:C15H14BrNO2
- Molecular Weight:320.18
51934-41-9
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$6.00/5g
586-78-7
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$14.00/5g
458550-44-2
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$154.00/0.25/ G
Yield:458550-44-2 73%
Reaction Conditions:
Stage #1: 4-iodobenzoic acid ethyl esterwith isopropylmagnesium chloride in tetrahydrofuran at -20; for 0.5 h;
Stage #2: para-nitrophenyl bromide in tetrahydrofuran at -20; for 2 h;
Stage #3: with sodium tetrahydroborate;iron(II) chloride in tetrahydrofuran;ethanol at 20; for 2 h;Further stages.;
References:
Sapountzis, Ioannis;Knochel, Paul [Journal of the American Chemical Society,2002,vol. 124,# 32,p. 9390 - 9391]
51934-41-9
292 suppliers
$6.00/5g
458550-44-2
28 suppliers
$154.00/0.25/ G
![Benzoic acid, 4-[bis(trimethylsilyl)amino]-, ethyl ester](/CAS/20210305/GIF/111017-08-4.gif)
111017-08-4
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458550-44-2
28 suppliers
$154.00/0.25/ G
94-09-7
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$5.00/50mg
458550-44-2
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$154.00/0.25/ G
106-40-1
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$12.00/5g
458550-44-2
28 suppliers
$154.00/0.25/ G