N-(4-CHLOROPHENYL)-2-NITROBENZENAMINE synthesis
- Product Name:N-(4-CHLOROPHENYL)-2-NITROBENZENAMINE
- CAS Number:23008-56-2
- Molecular formula:C12H9ClN2O2
- Molecular Weight:248.67
106-47-8
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23008-56-2
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Yield:23008-56-2 96%
Reaction Conditions:
with triethylamine in neat (no solvent) at 140; for 9 h;
Steps:
General procedure for the synthesis of 3 in Table 3
General procedure: A mixture of 1-fluoro-2-nitrobenzene 1 (1.5 g, 11 mmol), 2 (16 mmol), and triethylamine (0.6 g, 5.5 mol) was stirred at 140 °C for 9 h. After completion of the reaction as indicated by TLC, the mixture was cooled to 20 °C and filtered. The filter cake was washed with water and anhydrous ethanol until the pH of filtrate reached 7, then dried in vacuum to obtain compound 3.
References:
Cui, Jian-Lan;Wang, Ning;Wang, Xiao;Yu, Si-Yuan;Zhong, Cong-Shan [Tetrahedron Letters,2020,vol. 61,# 11] Location in patent:supporting information
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5570-19-4
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127-09-3
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23008-56-2
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$10.00/250mg