Pentamethylcyclopentadienyltitanium trichloride synthesis
- Product Name:Pentamethylcyclopentadienyltitanium trichloride
- CAS Number:12129-06-5
- Molecular formula:C10H15Cl3Ti
- Molecular Weight:289.45
![Silicon, trimethyl[(1,2,3,4,5-η)-1,2,3,4,5-pentamethyl-2,4-cyclopentadien-1-yl]-](/CAS/20211123/GIF/136990-69-7.gif)
136990-69-7
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7550-45-0
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75-77-4
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12129-06-5
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Yield:12129-06-5 99%
Reaction Conditions:
in toluene;Dropwise addn. of TiCl4 in toluene to soln. of C(CH3)5Si(CH3)3 in toluene (N2), stirring (2 h, color change from red-orange to red).; Evapn. of solvent and byproduct (vacuum), washing of crystals (pentane), dried (vacuum), elem. anal.;
References:
Llinas, Gerardo Hidalgo;Mena, Miguel;Palacios, Federico;Royo, Pascual;Serrano, Ricardo [Journal of Organometallic Chemistry,1988,vol. 340,p. 37 - 40]
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87778-95-8
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12129-06-5
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![Titanium, [μ-[methylene[(1,2,3,4,5-η)-2,3,4,5-tetramethyl-2,4-cyclopentadien-1-ylidene]]]di-μ-oxobis[(1,2,3,4,5-η)-1,2,3,4,5-pentamethyl-2,4-cyclopentadien-1-yl]di- (9CI)](/CAS/20211123/GIF/76586-30-6.gif)
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12129-06-5
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11136-36-0
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4045-44-7
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7550-45-0
336 suppliers
$10.00/10g
12129-06-5
114 suppliers
$30.00/250mg