PRISTANE synthesis
- Product Name:PRISTANE
- CAS Number:1921-70-6
- Molecular formula:C19H40
- Molecular Weight:268.52
505-32-8
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1921-70-6
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Yield:-
Steps:
Multi-step reaction with 5 steps
1: sodium periodate; acetic acid / acetone / 8 h / 80 °C
2: tetrahydrofuran / 1 h / -10 - 20 °C / Inert atmosphere
3: triethylamine / dichloromethane / 2 h / 20 °C / Cooling with ice
4: potassium bromide / acetone / 12 h / 100 °C
5: zinc borohydride / tetrahydrofuran / 12 h / 20 °C / Cooling with ice
References:
Yang Chaowen CN105016951, 2016, B
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1921-70-6
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253686-88-3
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502-69-2
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1921-70-6
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1921-70-6
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