Z-D-ALA-D-ALA-OME synthesis
- Product Name:Z-D-ALA-D-ALA-OME
- CAS Number:19914-26-2
- Molecular formula:C15H20N2O5
- Molecular Weight:308.33
26607-51-2
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14316-06-4
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19914-26-2
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Yield:19914-26-2 88%
Reaction Conditions:
Stage #1: N-benzyloxycarbonyl-D-alaninewith benzotriazol-1-ol;1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in tetrahydrofuran at 20; for 0.5 h;Inert atmosphere;
Stage #2: D-alanine methyl ester hydrochloridewith N-ethyl-N,N-diisopropylamine in tetrahydrofuran at 20; for 21 h;Inert atmosphere;
References:
Wohnig, Stephanie;Spork, Anatol P.;Koppermann, Stefan;Mieskes, Gottfried;Gisch, Nicolas;Jahn, Reinhard;Ducho, Christian [Chemistry - A European Journal,2016,vol. 22,# 49,p. 17813 - 17819] Location in patent:supporting information
![Alanine, N-[(phenylmethoxy)carbonyl]alanyl-, methyl ester (9CI)](/CAS/20210305/GIF/22221-78-9.gif)
