N-氰乙基哌啶(3088-41-3)紅外圖譜(IR1)

產(chǎn)品名稱:N-氰乙基哌啶

CAS:3088-41-3

分子式:C8H14N2

分子量: 138.21

InChI:InChI=1S/C8H14N2/c9-5-4-8-10-6-2-1-3-7-10/h1-4,6-8H2

InChIKey: YZICFVIUVMCCOC-UHFFFAOYSA-N

Smiles:N1(CCC#N)CCCCC1

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-7604          
1-piperidinepropionitrile
C8H14N2             (Mass of molecular ion:    138)

   Source Temperature: 250 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      15.0       1.8
      18.0       1.1
      26.0       3.8
      27.0       6.4
      28.0       7.0
      29.0       3.7
      30.0       3.8
      39.0       4.9
      40.0       2.0
      41.0      16.2
      42.0      21.4
      43.0       3.0
      44.0       7.1
      51.0       1.9
      52.0       4.4
      53.0       5.0
      54.0       7.3
      55.0      14.6
      56.0       4.5
      57.0       2.7
      67.0       1.3
      68.0       1.8
      69.0       5.1
      70.0       4.4
      79.0       1.7
      81.0       1.3
      82.0       1.8
      83.0       2.8
      84.0       4.7
      85.0       2.0
      96.0       4.6
      97.0       2.2
      98.0     100.0
      99.0       7.1
     109.0       1.0
     137.0       3.0
     138.0       2.8

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₈ H₁₄ N₂	0.05 ml : 0.5 ml CDCl₃
1-piperidinepropionitrile

    Assign.     Shift(ppm)

      A             2.660
      B             2.504
      C             2.428
      D             1.582
      E             1.433

     Hz     ppm     Int.

   1071.17   2.681    432
   1070.31   2.679    460
   1067.50   2.672     89
   1063.23   2.661   1000
   1058.84   2.650     92
   1056.76   2.645    665
   1056.15   2.643    711
   1017.70   2.547     30
   1007.93   2.523    697
   1007.32   2.521    719
   1000.98   2.505    985
   1000.24   2.503    861
    996.70   2.494     94
    993.77   2.487    465
    993.04   2.485    480
    988.77   2.475     62
    987.79   2.472     62
    975.71   2.442    518
    970.58   2.429    694
    965.33   2.416    550
    643.92   1.612    274
    638.06   1.597    532
    632.32   1.583    787
    626.71   1.569    674
    621.34   1.555    356
    583.86   1.461    160
    577.88   1.446    300
    572.27   1.432    369
    566.41   1.418    209
    561.04   1.404     86

in CDCl3