(R)-1-(4-甲基苯基)乙胺(4187-38-6)質(zhì)譜(MS)

產(chǎn)品名稱:(R)-1-(4-甲基苯基)乙胺

CAS:4187-38-6

分子式:C9H13N

分子量: 135.21

InChI:InChI=1/C9H13N/c1-7-3-5-9(6-4-7)8(2)10/h3-6,8H,10H2,1-2H3/t8-/s3

InChIKey: UZDDXUMOXKDXNE-SBYBRXNCNA-N

Smiles:[C@@H](C1C=CC(C)=CC=1)(N)C |&1:0,r|

¹HNMR

IR1

Mass

MS-IW-4067          
(R)-(+)-1-(p-tolyl)ethylamine
C9H13N              (Mass of molecular ion:    135)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      28.0       5.6
      39.0       2.6
      41.0       1.5
      42.0       9.1
      43.0       5.4
      44.0       9.5
      51.0       2.0
      58.5       1.4
      59.5       5.6
      60.0       3.1
      63.0       1.6
      65.0       5.0
      66.5       1.7
      77.0       9.2
      78.0       1.7
      79.0       1.1
      89.0       1.6
      91.0      17.5
      92.0       3.2
      93.0      25.7
      94.0       2.0
     103.0       1.1
     115.0       2.1
     117.0       3.6
     118.0       5.6
     119.0       5.9
     120.0     100.0
     121.0       9.2
     134.0       6.0
     135.0       2.9

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₉ H₁₃ N	0.05 ml : 0.5 ml CDCl₃
(R)-(+)-1-(p-tolyl)ethylamine

    Assign.     Shift(ppm)

      A             7.200
      B             7.109
      C             4.034
      D             2.303
      E             1.53
      F             1.336

     Hz     ppm     Int.

   2882.32   7.213    322
   2874.27   7.192    460
   2844.36   7.118    386
   2836.55   7.098    277
   1622.19   4.060     54
   1615.60   4.043    157
   1609.01   4.027    159
   1602.42   4.010     58
    920.65   2.304   1000
    612.30   1.533    175
    540.41   1.353     73
    537.60   1.346    861
    533.81   1.336     73
    530.88   1.329    854

liquid film