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返回ChemicalBook首頁>CAS數(shù)據(jù)庫列表>4232-27-3更多圖譜> 2,4-二硝基苯酯(4232-27-3)核磁圖(1HNMR)

4232-27-3

2,4-二硝基苯酯(4232-27-3)核磁圖(1HNMR)

產(chǎn)品名稱:2,4-二硝基苯酯

CAS:4232-27-3

分子式:C8H6N2O6

分子量: 226.14

  • 圖譜
    Mass 

    MS-IW-3902          
2,4-dinitrophenyl acetate
C8H6N2O6            (Mass of molecular ion:    226)


       Source Temperature: 120 °C
   Sample Temperature: 110 °C
   Direct, 75 eV


          15.0       2.2
      28.0       1.4
      30.0       2.4
      38.0       1.3
      42.0       4.2
      43.0     100.0
      44.0       4.2
      50.0       1.1
      51.0       2.6
      53.0       2.8
      61.0       1.1
      62.0       4.3
      63.0       8.1
      64.0       1.6
      74.0       1.1
      79.0       2.0
      91.0       3.0
      92.0       2.0
      93.0       1.2
     107.0       1.9
     154.0       1.4
     168.0       1.4
     184.0       4.6
     226.0       3.8

400 MHz in CDCl3

  • 圖譜

    1H NMR 399.65 MHz
    C8 H6 N2 O6 0.041 g : 0.5 ml CDCl3
    2,4-dinitrophenyl acetate
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             8.960
      B             8.534
      C             7.502
      D             2.434
     
     J(A,B)=2.7HZ
     J(A,C)=0.4HZ
     J(B,C)=8.9HZ
  

         Hz     ppm     Int.


       3582.52   8.965    134
   3579.83   8.958    142
   3416.63   8.550    106
   3413.94   8.543    105
   3407.71   8.527    111
   3405.03   8.521    111
   3002.69   7.514    152
   2993.77   7.491    147
    973.02   2.435   1000
    969.12   2.425     27

in CDCl3

  • 圖譜

KBr disc

  • 圖譜

nujol mull

  • 圖譜

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