17096-07-0
中文名稱
甲基丙烯酰氧丙基三(三甲基硅氧烷基)硅烷
英文名稱
3-(METHACRYLOYLOXY)PROPYLTRIS(TRIMETHYLSILOXY)SILANE
CAS
17096-07-0
EINECS 編號(hào)
241-165-0
分子式
C16H38O5Si4
MDL 編號(hào)
MFCD00053871
分子量
422.81
MOL 文件
17096-07-0.mol
更新日期
2025/08/11 15:40:43
17096-07-0 結(jié)構(gòu)式
基本信息
中文別名
3-甲基丙烯酸丙基三(三甲氧基硅)甲基丙烯酰氧丙基三(三甲基硅氧烷基)硅烷
3-(異丁烯酰氧)丙基三(三甲基硅氧烷)硅烷
3-(異丁烯酰氧)丙基三(三甲基硅氧基)硅烷
3-甲基丙烯酰氧丙基三(三甲基硅氧基)硅烷
英文別名
3-METHACRYLOXYPROPYLTRIS(TRIMETHYLSILOXY)SILANE3-(METHACRYLOYLOXY)PROPYLTRIS(TRIMETHYLSILOXY)SILANE
3-METHACRYLOYLOXYPROPYLTRIS-(TRIMETHYLSILYLOXY)-SILAN
3-(METHACRYLOYLOXY)PROPYLTRIS(TRIMETHYLSILYLOXY)SILANE
3-[TRIS(TRIMETHYLSILOXY)SILYL]PROPYL METHACRYLATE
3-[TRIS(TRIMETHYLSILYLOXY)SILYL]PROPYL METHACRYLATE
METHACRYLIC ACID 3-[TRIS(TRIMETHYLSILYLOXY)SILYL]PROPYL ESTER
METHACRYLOXYPROPYLTRIS(TRIMETHYLSILOXY)SILANE
TRIS(TRIMETHYLSILOXY)-3-METHACRYLOXYPROPYLSILANE
2-Propenoic acid, 2-methyl-, 3-[3,3,3-trimethyl-1,1-bis[(trimethylsilyl)oxy]disiloxanyl]propyl ester
3-[3,3,3-trimethyl-1,1-bis[(trimethylsilyl)oxy]disiloxanyl]propyl methacrylate
Tris(trimethylsiloxy)-3-methacryloxypropylsilane+6%Dimer
Tris(trimethylsiloxy)-3-methacryloxypropylsilane(3-Methacryloxypropyltris(trimethylsiloxy)silane)
Tris(trimethylsiloxy)-3-methacryloxypropylsilane+20%Dimer
3-Methacryloxypropyletris(trimethylsiloxy)silane
METHACRYLOXYPROPYLTRIS(TRIMETHYLSILOXY)SILANE: 80%, CONTAINS 20% SIB1400.0
METHACRYLOXYPROPYLTRIS(TRIMETHYLSILOXY)SILANE: 6% DIMER SIB1400
Tris(trimethylsiloxy)silylpropylmethacrylate
Methacrylic acid 4,4-bis(trimethylsilyloxy)-6,6-dimethyl-5-oxa-4,6-disilaheptane-1-yl ester
Methacrylic acid=3-[tris(trimethylsiloxy)silyl]propyl ester
所屬類別
化學(xué)試劑：硅烷物理化學(xué)性質(zhì)
熔點(diǎn)<0°C
沸點(diǎn)112-115 °C0.2 mm Hg(lit.)
密度0.918 g/mL at 25 °C(lit.)
蒸氣壓<1 mm Hg ( 20 °C)
折射率n20/D 1.419(lit.)
閃點(diǎn)>230 °F
儲(chǔ)存條件below 5° C
形態(tài)透明液體
比重0.918
顏色無色至幾乎無色
水溶解性Immiscible with water.
BRN1888727
InChIKeyBESKSSIEODQWBP-UHFFFAOYSA-N
LogP9 at 20℃
CAS 數(shù)據(jù)庫17096-07-0(CAS DataBase Reference)
NIST化學(xué)物質(zhì)信息Tris(trimethylsiloxy)-3-methacryloxypropylsilane(17096-07-0)
安全數(shù)據(jù)
警示詞警告
危險(xiǎn)性描述H315-H319-H335
危險(xiǎn)品標(biāo)志Xi
危險(xiǎn)類別碼R36/37/38
安全說明S26-S36
WGK Germany3
F10
TSCANo
海關(guān)編碼29319090
制備方法
方法1
2754-27-0
2530-85-0
17096-07-0
向裝有恒壓滴液漏斗、磁力攪拌器、Dean-Stark分水器和冷凝管的500 mL三頸燒瓶中，在氮?dú)獗Ｗo(hù)下加入124.18 g (0.5 mol) 3-(甲基丙烯酰氧)丙基三甲氧基硅烷，隨后加入0.15 g三氟甲磺酸和0.15 g BHT。通過恒壓滴液漏斗在80°C下緩慢滴加198.35 g (1.5 mol)三甲基硅乙酸酯至反應(yīng)燒瓶中。滴加過程中，大部分低沸點(diǎn)副產(chǎn)物通過Dean-Stark分水器側(cè)管連續(xù)蒸餾并收集。滴加完畢后，繼續(xù)攪拌反應(yīng)混合物1小時(shí)。將反應(yīng)混合物轉(zhuǎn)移至分液漏斗中，用100 mL水洗滌六次，直至獲得中性無色透明液體。通過減壓旋轉(zhuǎn)蒸發(fā)去除少量低沸點(diǎn)雜質(zhì)，最終得到198.08 g 3-(1,1,1,5,5,5-六甲基-3-((三甲基硅基)氧基)三硅氧烷-3-基)甲基丙烯酸丙酯，產(chǎn)率為93.7%。
參考文獻(xiàn)：
[1] Patent: CN103554169, 2016, B. Location in patent: Paragraph 0040-0042
知名試劑公司產(chǎn)品信息
Alfa Aesar
3-(異丁烯酰氧）丙基三(三甲基硅氧烷)硅烷,98%3-(Methacryloyloxy)propyltris(trimethylsiloxy)silane, 98%(17096-07-0)
Sigma Aldrich
17096-07-0(sigmaaldrich)甲基丙烯酰氧丙基三(三甲基硅氧烷基)硅烷價(jià)格(試劑級(jí))
| 報(bào)價(jià)日期 | 產(chǎn)品編號(hào) | 產(chǎn)品名稱 | CAS號(hào) | 包裝 | 價(jià)格 |
| 2025/05/22 | L16682 | 3-(異丁烯酰氧)丙基三(三甲基硅氧烷)硅烷, 98% 3-(Methacryloyloxy)propyltris(trimethylsiloxy)silane, 98% | 17096-07-0 | 25g | 673元 |
| 2025/05/22 | L16682 | 3-(異丁烯酰氧)丙基三(三甲基硅氧烷)硅烷, 98% 3-(Methacryloyloxy)propyltris(trimethylsiloxy)silane, 98% | 17096-07-0 | 100g | 2010元 |
| 2025/05/22 | M1324 | 甲基丙烯酸3-[三(三甲基硅氧基)甲硅烷基]丙酯 3-[Tris(trimethylsilyloxy)silyl]propyl Methacrylate | 17096-07-0 | 25ML | 700元 |